1-Phenyl-3-{4-[4-(4-undecyloxybenzoyloxy)phenyloxycarbonyl]phenyl}triazene 1-oxide

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1-Phenyl-3-{4-[4-(4-undecyl­oxybenzoyl­oxy)phenyl­oxycarbon­yl]phen­yl}triazene 1-oxide

The X-ray crystallographic study of the title compound, C(37)H(41)N(3)O(6), at 150 K establishes the N-oxide form of the triazene 1-oxide unit. There is one intra-molecular N-H⋯O hydrogen-bonding inter-action and the crystal packing is stabilized by one N-H⋯O, three C-H⋯O and three C-H⋯π inter-molecular inter-actions. The dihedral angles between pairs of adjacent benzene rings are 14.9 (3), 56....

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Synthesis and Antimicrobial Activity of Some 2-[(4-Substituted-Phenyl-3-Chloro-Azetidin-2-One)-5-(2'-Methylamino-4-Phenyl-1', 3'-Thiazolyl-]-1, 3,4-Thiadiazoles

A new 2-[(4-substituted-phenyl-3-chloroazetidin-2-one)-5-(2'-methylamino 4-phenyl-1', 3'-thiazolyl-]-1, 3, 4-thiadiazoles, 5(a-n) were synthesized from 2-substituted-benzylideneamino-5-[2'-methylamino-4'-phenyl-1',3'-thiazolyl]-1,3, 4-thiadiazole, 4(a-n) using 2-amino-4phenyl-1, 3-thiazole as a starting material. The synthesised compounds have been screened in vitro for their antimicrobial acti...

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4-(4-Fluoro­benzo­yl)-3-phenyl-3,4-di­hydro­naphthalen-1(2H)-one

In the title compound, C23H17FO2, the cyclo-hexenone ring has an envelope conformation, the flap atom being the C atom to which the phenyl ring is attached. The 4-fluoro-benzoyl ring and the phenyl ring are inclined to one another by 28.77 (7)°, and by 52.00 (7) and 44.77 (7) °, respectively, to the aromatic ring fused to the cyclo-hexenone ring. In the crystal, mol-ecules are linked via C-H⋯O ...

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3-(4-Meth­oxy­phen­yl)-1-phenyl-1H-pyrazole-4-carbaldehyde

Four independent mol-ecules comprise the asymmetric unit of the title compound, C(17)H(14)N(2)O(2). The central pyrazoline ring is flanked by an N-bound benzene ring and a C-bound meth-oxy-substituted benzene ring. The greatest difference between the independent mol-ecules is found in the relative orientations of the benzene rings with the range of dihedral angles being 23.59 (6)-42.55 (6)°. In...

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3-(4-Bromo­phen­yl)-1-phenyl-1H-pyrazole-4-carbaldehyde

In the title compound, C(16)H(11)BrN(2)O, the phenyl and chloro-benzene rings are twisted out of the mean plane of the pyrazole ring, forming dihedral angles of 13.70 (10) and 36.48 (10)°, respectively. The carbaldehyde group is also twisted out of the pyrazole plane [the C-C-C-O torsion angle is 7.9 (3)°]. A helical supra-molecular chain along the b axis and mediated by C-H⋯O inter-actions is ...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2008

ISSN: 1600-5368

DOI: 10.1107/s1600536808005904